CHLOROPHYLL-A CONCENTRATIONS IN LAKES OF THE MCMURDO DRY VALLEY


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CHLOROPHYLL-A CONCENTRATIONS IN LAKES OF THE MCMURDO DRY VALLEY
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PRINCIPAL INVESTIGATOR: John Priscu
Address:Department of Biology, Montana State University, Bozeman MT, 59717
Phone:(406)994-3250
E-Mail:ubijp@gemini.oscs.montana.edu or JPriscu@LTERnet.edu

KEYWORDS: lake, limnology, primary production, chlorophyll-a, Antarctica

ABSTRACT: An important part of the McMurdo Long Term Ecological Research (LTER) project is monitoring of spatial and temporal patterns, and processes that control primary production in perennial ice-covered lakes. This data set addresses this core area of research and quantifies chlorophyll-a concentrations at specific depths in McMurdo Dry Valley lakes.

VARIABLES: limno run, location name, location code, date, depth (m), Chl-a (µg L-1), Chl-a comments, file name

RESEARCH LOCATION: Samples were collected from the East Lake Bonney, West Lake Bonney, Lake Hoare, Lake Fryxell, Lake Joyce, and Lake Miers limnological sampling stations, located in the McMurdo Dry Valleys of Antarctica. Descriptions of these lakes can be found in the McMurdo Dry Valley Lake Descriptions file.

METHODS: Lake water samples were collected at specific depths with a five-liter Niskin bottle during normal LTER limnological sampling. Sub-samples were decanted into three-1 L Nalgene bottles (2-light and 1-amber), two-500 mL amber Nalgene bottles, three-150 mL borosilicate glass bottles, two-20 mL scintillation vials, and one-30 mL serum vial. Two-100 mL sub-samples were taken from the one-liter amber Nalgene bottle. In a darkened environment, each sample was filtered through a combusted (475°C for 4 hours) Whatman 25 mm GF/F using a bell jar apparatus. The filter was folded in half (organic material inside), placed in a glassine envelope, covered with aluminum foil, and frozen immediately for later analysis in McMurdo. The filtrate was collected for nutrient and dissolved organic carbon analyses.

In McMurdo, chlorophyll-a standards were prepared by dissolving 1 mg of chlorophyll-a in a 100 ml volumetric flask and diluting it to mark with a 1:1 solution of 90% acetone and DMSO. A Beckman DU-640 UV/vis spectrophotometer was used to determine the actual stock concentration. The absorbance of the stock solution was determined at l=665 nm and l=750 nm; The corrected initial absorbance was calculated (665o = Abs.665 - Abs.750). The stock solution was acidified in the cuvette using 4 drops of 3 N HCl and analyzed again. The absorbance after acidification was used at l=665 nm and l=750 nm to determine 665a (665a = Abs.665 - Abs.750). Chlorophyll-a content was determined by the following equation:

Chl-a = 26.7 x (665o - 665a) x v
V * L

where v = extract volume, V = volume of water filtered, and L is the pathlength of the cuvette. The stock solution was used to prepare six standard solutions of chlorophyll-a ranging from ~ 0.0015 µg ml-1 to 0.150 µg ml-1. Fo and Fa were obtained for each standard by collecting initial fluorescence data, and then acidifying the standard in the cuvette with 4 drops of 3 N HCl. The cuvette was briefly vortexed before determining Fa.

Each filter was placed into a 20 ml scintillation vial and extracted with 10 ml of 1:1 solution of 90% acetone and DMSO. The extract was incubated for ~12 hours under cold (<0°C), dark conditions. After incubation, 4 ml of extract was briefly vortexed & dispensed into the cuvette; the cuvette was inserted into the Turner 10-AU fluorometer. After Fo was determined, the sample was acidified with 4 drops of 3 N HCl, vortexed, and Fa was determined. The cuvette was rinsed three times with DI water and three times with 90% acetone to ensure there was no cross contamination between samples. The cuvette exterior was wiped with Kimwipes. The Fo-Fa was determined for each sample and chlorophyll-a concentration was calculated using the standard curve.

TIMING: Samples were collected from the following sites and dates:


 
Season		East Bonney	West Bonney	Hoare		Fryxell		Joyce		Miers		Trough
1993-1994	27-Oct-1993	29-Oct-1993	 6-Nov-1993	16-Nov-1993
 		10-Nov-1993	12-Nov-1993
 		24-Nov-1993	26-Nov-1993	 1-Dec-1993	 7-Dec-1993
 		 7-Dec-1993	 9-Dec-1993
 		21-Dec-1993	23-Dec-1993	30-Dec-1993	 7-Jan-1994
 						19-Jan-1994	18-Jan-1994
 													
1994-1995	 2-Nov-1994	 5-Nov-1994	10-Nov-1994	14-Nov-1994
 		23-Nov-1994	25-Nov-1994	30-Nov-1994	 4-Dec-1994
 		17-Dec-1994	19-Dec-1994	24-Dec-1994	30-Dec-1994
 		10-Jan-1995	12-Jan-1995	20-Jan-1995	17-Jan-1995
 		
1995-1996	19-Sep-1995	21-Sep-1995	 7-Sep-1995	14-Sep-1995
 						14-Sep-1995
 		 6-Oct-1995	 4-Oct-1995	25-Sep-1995	28-Sep-1995
 		17-Oct-1995	19-Oct-1995	10-Oct-1995	14-Oct-1995
 		 2-Dec-1995	 5-Dec-1995	21-Nov-1995	26-Nov-1995
 		 1-Jan-1996	 4-Jan-1996	23-Dec-1995	27-Dec-1995
 		
1996-1997	 3-Nov-1996	 1-Nov-1996	 8-Nov-1996	26-Oct-1996
 		24-Nov-1996	26-Nov-1996	 2-Dec-1996	19-Nov-1996	5-Dec-1996	10-Dec-1996
 		15-Jan-1997	17-Jan-1997	12-Jan-1997	 9-Jan-1997

1997-1998	 				31-Oct-1997	 2-Nov-1997
 		 8-Nov-1997	11-Nov-1997	 7-Nov-1997	12-Nov-1997			
 		 				15-Nov-1997	18-Nov-1997
 		 1-Dec-1997			26-Nov-1997	28-Nov-1997
 		 8-Dec-1997	 3-Dec-1997	10-Dec-1997	 5-Dec-1997	9-Dec-1997	 5-Dec-1997
 						12-Dec-1997	16-Dec-1997
 		20-Dec-1997	22-Dec-1997	26-Dec-1997	29-Dec-1997
 						 6-Jan-1998	 8-Jan-1998
 						17-Jan-1998	20-Jan-1998
 						26-Jan-1998 

1998-1999	 9-Nov-1998	11-Nov-1998	 3-Nov-1998	28-Oct-1998					
		 6-Dec-1998	 9-Dec-1998 	 1-Dec-1998	23-Nov-1998
		30-Dec-1998	 1-Jan-1999	26-Dec-1998	20-Dec-1998					23-Dec-1998

1999-2000	 6-Nov-1999	11-Nov-1999	17-Nov-1999	30-Oct-1999
		 3-Dec-1999	 5-Dec-1999	12-Dec-1999	27-Nov-1999
		28-Dec-1999	30-Dec-1999	 4-Jan-2000	23-Dec-1999


CITATIONS: Holm-Hansen, O., C. J. Lorenzen, R. W. Holmes, and J. D. H. Strickland. 1965. Fluorometric determination of chlorophyll. J. Cons. Int. Explor. Mer. 30: 3-15.

Strickland, J.D.H. and Parsons. 1977. A practical handbook of seawater analysis. pg. 194.

COMMENTS: Chlorophyll-a values reported in this file are the means of two replicate samples taken at each depth.

STATUS: Public Access (Type 1).

VARIABLE DESCRIPTION:

VARIABLE

TYPE

DESCRIPTION

UNITS

MISSING VALUE INDICATOR

MINIMUM

MAXIMUM

PRECISION

Limno Run

Text

Code for lake's sampling location and date

none

Required entry

n/a

n/a

n/a

Location Name

Text

Name of lake where measurement was made

none

Required entry

n/a

n/a

n/a

Location Code

Text

Code for site where measurement was made

none

Required entry

n/a

n/a

n/a

Date

Date

Date on which sample was gathered

mm/dd/yy

Required entry

01/01/93

12/31/99

dd

Depth (m)

Number

Distance below ice from which sample was drawn

meters

Required entry

1

60

1

CHL (µg chl a/l)

Number

Chlorophyll a concentration, as averaged from 2 replicates, and measured by Turner Designs Fluorometer

µg Chlorophyll-a/liter

Null

-1

25

0.001

CHL Comments

Text

Helpful hints about the sample

none

Null

n/a

n/a

n/a

File Name

Text

Name of file in which data was submitted

none

Null

n/a

n/a

n/a

LOG: Data from this table was submitted to INSTAAR by John Priscu's team at Montana State University. The raw data files listed under 'file name' are the names of the original files submitted. The 1993/94 and 1994/95 datasets are Microsoft Excel version 6.0 files, and the 1995/96, 1996/97 and 1997/98 datasets are ascii text files.

Upon arrival at INSTAAR, the data manager fine-tuned the location codes and limno runs to match those provided in the "locations, dates, codes for lake chemistry, biology samples" file. The file was imported into Microsoft Access on INSTAAR's Unix system, and can currently be found there. The file was then exported in ascii, comma delimited text and MS-DOS text (table layout) on the MCM LTER web site. Both of these files are linked to this web page above.

Information for the metadata was obtained from the Metachl9697.rtf file. The file was called up using Microsoft Word version 6.0. Text from this file was used to create this page in html format.

NOTE: Data contained in these files has been subjected to quality control standards imposed by the investigator. The user of this data should be aware that, while efforts have been taken to ensure that these data are of the highest quality, there is no guarantee of perfection for the data contained herein and the possibility of errors exists. If you encounter questionable data, please contact the MCM LTER data manager (; (303)492-4639) so that the data can be corrected or qualified. Thus, these data may be modified and future data will be appended.